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A [TEACOOH]-Montmorillonite intercalations complex obtained from Na-Montmorillonite and 10-Carboxy-n-triethylammo-ε-caprolactone between the layer spaces of the intercalations complex toachieve Montmorillonite-Polycaprolactone nanocomposites in which the inorganic material (montmorillonite) is chemically com-bined with the organic polymer (polycaprolactone). The results of X-ray-, IR-, and TEM-analyses for samples obtained after poly-merization showed that a polycondensation reaction was successfuly produced. For a more precise investigation of the polymericreaction products the polymerized products were separated from the silicate layers and analyzed with an IR-spectrometer. A com-parison of the results of the IR-analyses of the separated polymer with that of the polymer synthesized by the reaction of ε-capro-compound.